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Ultra-fast determination of base metals in geochemical samples using the 5100 SVDV ICP-OES
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2024-09-29 22:17 502閱讀次數(shù)
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Traditionally, geological samples are analyzed using flame atomic absorption (FAAS) and/or radial ICP-OES with a vertical torch. Achieving high sample throughput at a low cost per analysis for geochemical samples can be challenging when using these techniques.
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Ultra-fast determination of base metals in geochemical samples using the 5100 SVDV ICP-OES Traditionally, geological samples are analyzed using flame atomic absorption (FAAS) and/or radial ICP-OES with a vertical torch. Achieving high sample throughput at a low cost per analysis for geochemical samples can be challenging when using these techniques. [詳細(xì)]
2024-09-29 22:17
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O, N determination in titanium samples SuitableanalyzersnON900nONH2000UsedaccessoriesnInnergraphitecrucibles(90180)nOutergraphitecrucibles(90185)nNickelbasket(90250)orAR2344nSuitablecalibrationmaterial(NISTorother)SettingsnComparatorlevel:20mVnMinimumtime:15secnMaximumtime:3:00minnPostwaiting:30secnBaselinedeviation:200mV;Step:16mV;Time:10secnMode:continuousnOutgasTime:45secPower:6kWnTimePurge:20secStability:45secnIntegrationdelayIRcell:2secTCcell:10secnAnalyse(1)Time:75secPower(1):6kWPower(2):6kWSamplepreparationMakesurethatthesurfaceofthetitaniumisfreefromcontaminations;otherwisecleanthesamplewithacetonep.a.andletdryatatmosphere.ProcedurenPrepareELTRAanalyzer(exchangeanhydrone,sodiumhydroxide,copperoxidewhennecessary),cleanfurnace,sampledropmechanism,electrodetipnRunthreeblankswithemptycruciblesnCalibratetheanalyzerwithsuitablecalibrationmaterial(NISTorother)(1)Filloneemptyinnercrucible(90180)inoneoutercrucible(90185)andplacethemontheelectrodetip,closefurnace(F2Button)(2)Weighcalibrationmaterialandgiveitintoanickelbasket(90250orAR2344)(3)Placenickelbasketwithcalibrationmaterialorsampleinthesampledropmechanismandstartanalysis(F5Button)Afteranalysisgivetheinnercrucibleintowasteandfillinanewone.Theoutercruciblescanbeusedapproximately10times.Repeatsteps(1)(3)atleastthreetimes;Marktheresultsandusethecalibrationfunctioninthesoftware.[詳細(xì)]
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O, N determination in steel samples (single graphite crucibles) SuitableanalyzersnON900nONH2000UsedaccessoriesnGraphitecrucibles(90190)nSuitablecalibrationmaterial(NISTorother)SettingsnComparatorlevel:5mV(lowoxygen);20mV(other)nMinimumtime:15sec(oxygen);35sec(nitrogen)nMaximumtime:3:00minnPostwaiting:20secnBaselinedeviation:20mV;Step:16mV;Time:10secnMode:continuousnOutgasTime:45secPower:5kWnTimePurge:15secStability:45secnIntegrationdelayIRcell:2secTCcell:10secnAnalyse(1)Time:40secPower(1):4kWPower(2):4kWSamplepreparationMakesurethatthesurfaceofthesteelisfreefromcontaminations;otherwisecleanthesamplewithacetonep.a.andletdryatatmosphere.ProcedurenPrepareELTRAanalyzer(exchangeanhydrone,sodiumhydroxide,copperoxidewhennecessary),cleanfurnace,sampledropmechanism,electrodetipnRunthreeblankswithemptycruciblesnCalibratetheanalyzerwithsuitablecalibrationmaterial(NISTorother)(1)Placeemptycrucible(90190)ontheelectrodetip,closefurnace(F2Button)(2)Weighcalibrationmaterial(usuallypins)(3)Placecalibrationmaterialinthesampledropmechanismandstartanalysis(F5Button)Repeatsteps(1)(3)atleastthreetimes;Marktheresultsandusethecalibrationfunctioninthesoftware.[詳細(xì)]
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Ultra-fast determination of base metals in geochemical samples using the 5100 SVDV ICP-OES
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