德國(guó)布魯克微區(qū)X射線熒光能譜儀M4 TORNADO
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小麥元素分布檢測(cè)-德國(guó)布魯克微區(qū)X射線熒光能譜儀M4TORNADOElementalDistributionExaminationonWheatSeedSamplesMeasurementConditionCustomerSampleObjective:ElementaldistributionexaminationofMn,Fe,Zn,Cu,Cd,P,S,Konwheatseedsamples(n=8,bothtransverseandlongitudinalsectionsfor4setsamples),asperreceived.LeftImage:Wheatseedsampleinnon-embedded,longitudinalandtransverseformrespectivelyRightImage:Samples(N=8)LoadingintotheM4SampleChamberAnalysisResult(a)HOSUT2–LongitudinalSectionCameraImage–10xmagnification(Left)andElementalMapping(Right)ofWheatSeedSample“HOSUT2Longitudinalsection”withcombinationofMn,Fe,Zn,Cu,Cd,P,SandKelement.IndividualElementalMappingofZn,FeandMnrespectivelyElementalMappingof(P+S),KandCurespectivelyAnalysisResult(b)HOSUT3–LongitudinalSectionCameraImage–10xmagnification(Left)andElementalMapping(Right)ofWheatSeedSample“HOSUT3Longitudinalsection”withcombinationofMn,Fe,Zn,Cu,P,SandKelement.IndividualPElementalMapping(Left)and“FalseColorDisplay”IndividualPElementalDistributionMapping(Right)onWheatSeed‘HOSUT3–LongitudinalSection’“FalseColorDisplay”:PhosphorusIntensitySaturationcorrelationineachmappingpixel.Forinstance,thered/blackareaiscorrelatedwithlow/nosulfurconcentration;Thephosphoruscontentisfoundhigherinblue/whiteareaascomparedtogreenarea,referringtotheintensitycolorindicatoronrightside.ElementalMappingof(K+S)and(Mn+Fe+Zn)respectivelyConclusionsAsdemonstrated,M4TornadoisabletoperformquickandnondestructivelyelementalmappinganalysisforexaminingvariouselementdistributiononwheatseedSamplesincludingthefollowingcapabilities:1.Highnumberofsamplesloadingatonetimewithlargesamplechamber2.VaryingElementalDistributionStudyincludingP,S,K,Mn,Fe,ZnandCuonwheatseedSamples3.“FalseColorDisplay”functionmodehelpsinelementdistributionexaminationtofurtherextent
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德國(guó)布魯克微區(qū)X射線熒光能譜儀M4 TORNADO- 小麥元素分布檢測(cè)-德國(guó)布魯克微區(qū)X射線熒光能譜儀M4TORNADOElementalDistributionExaminationonWheatSeedSamplesMeasurementConditionCustomerSampleObjective:ElementaldistributionexaminationofMn,Fe,Zn,Cu,Cd,P,S,Konwheatseedsamples(n=8,bothtransverseandlongitudinalsectionsfor4setsamples),asperreceived.LeftImage:Wheatseedsampleinnon-embedded,longitudinalandtransverseformrespectivelyRightImage:Samples(N=8)LoadingintotheM4SampleChamberAnalysisResult(a)HOSUT2–LongitudinalSectionCameraImage–10xmagnification(Left)andElementalMapping(Right)ofWheatSeedSample“HOSUT2Longitudinalsection”withcombinationofMn,Fe,Zn,Cu,Cd,P,SandKelement.IndividualElementalMappingofZn,FeandMnrespectivelyElementalMappingof(P+S),KandCurespectivelyAnalysisResult(b)HOSUT3–LongitudinalSectionCameraImage–10xmagnification(Left)andElementalMapping(Right)ofWheatSeedSample“HOSUT3Longitudinalsection”withcombinationofMn,Fe,Zn,Cu,P,SandKelement.IndividualPElementalMapping(Left)and“FalseColorDisplay”IndividualPElementalDistributionMapping(Right)onWheatSeed‘HOSUT3–LongitudinalSection’“FalseColorDisplay”:PhosphorusIntensitySaturationcorrelationineachmappingpixel.Forinstance,thered/blackareaiscorrelatedwithlow/nosulfurconcentration;Thephosphoruscontentisfoundhigherinblue/whiteareaascomparedtogreenarea,referringtotheintensitycolorindicatoronrightside.ElementalMappingof(K+S)and(Mn+Fe+Zn)respectivelyConclusionsAsdemonstrated,M4TornadoisabletoperformquickandnondestructivelyelementalmappinganalysisforexaminingvariouselementdistributiononwheatseedSamplesincludingthefollowingcapabilities:1.Highnumberofsamplesloadingatonetimewithlargesamplechamber2.VaryingElementalDistributionStudyincludingP,S,K,Mn,Fe,ZnandCuonwheatseedSamples3.“FalseColorDisplay”functionmodehelpsinelementdistributionexaminationtofurtherextent[詳細(xì)]
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2018-08-15 10:57
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- Stateoftheartmicro-XRFappliedtogeologicalsamplesMicro-XRFongeologicalsamplesM4TornadoLargesamples(H×W×D:200mm×160mm×120mm)Powerfulsamplestage(100mm/s,5kg)Pre-VacuumconditionsfordetectionofelementsdowntoNaPolycapillaryopticsforhighexcitationintensityandspotsize＜25μmSDDsfordetection/processingofover100kcpsVariousmeasurementmodes(single-ormulti-point,linescans,areascans)Optional2ndX-raytubeOptional2nddetectorPositionTaggedSpectroscopy(HyperMap)Versatile"data-mining"softwareStandard-freequantificationScanoftheCetaceous/PaleogeneboundaryinRatonBasinUSThinsectionsmeasurements(64-bitOS)TraceelementsingarentThinsectionofagarentcontainingslateFullareamapshowssymmetricMncorewithinthecrystalsSelectedgarnetneasuredextensivelywithstrongprimaryfiltertoreducebackgroundandtoavoidBraggdiffractionpeaks370pixel×460pixel→170000pixelmapMeasurementtime:1s/pixelSteps:25μmSummaryUniquespeedandperfoimanceinthedeterminationoftheelementdistributioninlargesamplewithmeasurementtiomesperpixelof0.3msanduptp4MillionpixelsinasingleHyperMapHighspatialresolutiondownto25μmX-rayspotsize,motorsstepsof4μmOptimalfortheanalysisofinhomogeneoussamples,duetobetteridentificationoftherepresentativelocationofinterestNon-destructive,fastanalysisoflargesampleswithoutpreparation,includingsolid,poweroeliquidsamplesQualitativeandquantitativeanalysisofallelementsfromNaupwards,duetovacuumchamber,detectionlimitforheavytraceelementsinthelowppmrangeStandardlessFundamentalParameterquantificationwithtypecalibrationoptionPowerfulSoftwarewithmultipletoolsforoptimaldatamining[詳細(xì)]
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- ElementalDistributionExaminationonPlantLeafSampleObjective:ElementaldistributionexaminationofCa,Co,K,NiandMnonfreeze-driedplantleafsamples(n=6),asperreceived.LeftImage:MosaicOverviewCameraImageofallsix(6)samplesRightImage:SamplesLoadingintotheM4SampleChamberAnalysisResult(a)PlantLeafSample1MosaicImage(Left)andElementalMapping(Right)ofPlantLeafSample1withcombinationofCa,Co,K,NiandMnIndividualElementalDistributionMappingofCaandMnrespectively(LefttoRight)onPlantLeafSample1IndividualElementalDistributionMappingofK,NiandCorespectively(LefttoRight)onPlantLeafSample1(b)PlantLeafSample2MosaicImage(Left)andElementalMapping(Right)ofPlantLeafSample2withcombinationofCa,Co,K,NiandMnMnElementalDistributionMappingonPlantLeafSample2CombinedSiandKElementalMapping(Left)andIndividualNiElementalDistributionMapping(Right)onPlantLeafSample2IndividualCaElementalMapping(Left)and“FalseColorDisplay"IndividualCaElementalDistributionMapping(Right)onPlantLeafSample2IndividualCoElementalDistributionMappingonPlantLeafSample2ConclusionsAsdemonstrated,M4Tornadoisabletoperformquickandnon-destructivelyelementalmappinganalysisforexaminingvariouselementdistributiononPlantLeafSamplesincludingthefollowingcapabilities:1.Highnumberofsamplesloadingatonetimewithlargesamplechamber2.VaryingPlantNutrientsElementalDistributionStudyincludingCa,Co,K,NiandMnonPlantLeafSampleswithminimalsamplepreparationefforts(Freeze-driedcondition,preparedbycustomerinthiscase)3.“FalseColorDisplay"functionmodehelpsinelementdistributionexaminationtofurtherextent[詳細(xì)]
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